Effect of different swelling agents on textural and structural properties of modified mesoporous silica
In this study was carried out the preparation of some large-pore ordered mesoporous silicas using a proper surfactant with different swelling agents. In order to use a micelle swelling agent with a moderate swelling ability we selected three swelling agents: 1-phenyldecane, butyl benzene and mesityl...
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Dokumentumtípus: | Könyv része |
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2019
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Sorozat: | Proceedings of the International Symposium on Analytical and Environmental Problems
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Kulcsszavak: | Kémia |
Online Access: | http://acta.bibl.u-szeged.hu/64832 |
LEADER | 02143naa a2200265 i 4500 | ||
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001 | acta64832 | ||
005 | 20220808153737.0 | ||
008 | 200319s2019 hu o 1|| zxx d | ||
020 | |a 978-963-306-702-4 | ||
040 | |a SZTE Egyetemi Kiadványok Repozitórium |b hun | ||
041 | |a zxx | ||
100 | 1 | |a Popa Alexandru | |
245 | 1 | 0 | |a Effect of different swelling agents on textural and structural properties of modified mesoporous silica |h [elektronikus dokumentum] / |c Popa Alexandru |
260 | |c 2019 | ||
300 | |a 226-230 | ||
490 | 0 | |a Proceedings of the International Symposium on Analytical and Environmental Problems | |
520 | 3 | |a In this study was carried out the preparation of some large-pore ordered mesoporous silicas using a proper surfactant with different swelling agents. In order to use a micelle swelling agent with a moderate swelling ability we selected three swelling agents: 1-phenyldecane, butyl benzene and mesitylene. The aim of these synthesis was to achieve a pore diameter enlargement but in the same time to avoid the formation of heterogeneous and/or poorly defined nanostructure of silica. These composites were characterized by FT-IR spectroscopy, X-ray diffraction at low angles, nitrogen physisorption at 77 K, SEM-EDS. In the view of a possible use of these amino-functionalized mesoporous silicas as adsorbents for CO2 removal, their adsorption– desorption properties towards CO2 were investigated by the TPD method. CO2 adsorption isotherms of amino-functionalized mesoporous silicas measured at 50, 60 and 70 °C showed that the adsorption capacity (mg CO2/g adsorbent) depend on the temperature of adsorption and on the type of swelling agents and amination reagents used. | |
695 | |a Kémia | ||
700 | 0 | 1 | |a Borcanescu Silvana |e aut |
700 | 0 | 1 | |a Barvinschi Paul |e aut |
700 | 0 | 2 | |a Bajuk-Bogdanović Danica |e aut |
700 | 0 | 2 | |a Uskoković-Marković Snežana |e aut |
700 | 0 | 2 | |a Holclajtner-Antunović Ivanka |e aut |
710 | |a International Symposium on Analytical and Environmental Problems (25.) (2019) (Szeged) | ||
856 | 4 | 0 | |u http://acta.bibl.u-szeged.hu/64832/1/proceedings_of_isaep_2019_226-230.pdf |z Dokumentum-elérés |