High-performance liquid chromatographic study on the enantioseparation of fluorine containing cyclic amino acid derivatives
The stereoisomers of several fluorinated cyclic β 3 -amino acid derivatives and their nonfluorinated counterparts were separated on chiral stationary phases containing as chiral selectors cellulose tris-(3,5-dimethylphenyl carbamate), cellulose tris-(3-chloro-4-methylphenyl carbamate), cellulose tri...
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| Dokumentumtípus: | Könyv része |
| Megjelent: |
2016
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| Sorozat: | Proceedings of the International Symposium on Analytical and Environmental Problems
22 |
| Kulcsszavak: | Analitikai kémia, Gyógyszerkémia |
| Online Access: | http://acta.bibl.u-szeged.hu/56129 |
| LEADER | 01952naa a2200289 i 4500 | ||
|---|---|---|---|
| 001 | acta56129 | ||
| 005 | 20220808154855.0 | ||
| 008 | 181213s2016 hu o 1|| zxx d | ||
| 020 | |a 978-963-306-507-5 | ||
| 040 | |a SZTE Egyetemi Kiadványok Repozitórium |b hun | ||
| 041 | |a zxx | ||
| 100 | 1 | |a Orosz Tímea | |
| 245 | 1 | 0 | |a High-performance liquid chromatographic study on the enantioseparation of fluorine containing cyclic amino acid derivatives |h [elektronikus dokumentum] / |c Orosz Tímea |
| 260 | |c 2016 | ||
| 300 | |a 399-401 | ||
| 490 | 0 | |a Proceedings of the International Symposium on Analytical and Environmental Problems |v 22 | |
| 520 | 3 | |a The stereoisomers of several fluorinated cyclic β 3 -amino acid derivatives and their nonfluorinated counterparts were separated on chiral stationary phases containing as chiral selectors cellulose tris-(3,5-dimethylphenyl carbamate), cellulose tris-(3-chloro-4-methylphenyl carbamate), cellulose tris-(4-methylbenzoate), cellulose tris-(4-chloro-3-methylphenyl carbamate), amylose tris-(3,5-dimethylphenyl carbamate) or amylose tris-(5-chloro-2-methylphenyl carbamate). The enantioseparations were carried out in normal-phase mode with n-hexane/alcohol/alkylamine mobile phases in the temperature range 5–40 °C. The effects of the mobile phase composition, the nature and concentration of the alcohol and alkylamine additives, the structures of the analytes and temperature on the separations were investigated. | |
| 695 | |a Analitikai kémia, Gyógyszerkémia | ||
| 700 | 0 | 1 | |a Lajkó Gyula |e aut |
| 700 | 0 | 1 | |a Grecsó Nóra |e aut |
| 700 | 0 | 1 | |a Kiss Lóránd |e aut |
| 700 | 0 | 1 | |a Forró Enikő |e aut |
| 700 | 0 | 1 | |a Fülöp Ferenc |e aut |
| 700 | 0 | 1 | |a Péter Antal |e aut |
| 700 | 0 | 1 | |a Ilisz István |e aut |
| 710 | |a International Symposium on Analytical and Environmental Problems (22.) (2016) (Szeged) | ||
| 856 | 4 | 0 | |u http://acta.bibl.u-szeged.hu/56129/1/proceedings_of_isaep_2016_399-401.pdf |z Dokumentum-elérés |