Polar pesticide analyses validation of glyphosate determination in soil by LC-MS/MS /
Although glyphosate is a heavily applied herbicide worldwide, the risk of environmental contamination through transport mechanisms of this substance is still not well documented and the methods for its analysis are usually very complex and nor sensitive enough. In the measurement procedure with LC-M...
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| Dokumentumtípus: | Könyv része |
| Megjelent: |
2016
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| Sorozat: | Proceedings of the International Symposium on Analytical and Environmental Problems
22 |
| Kulcsszavak: | Peszticid, Analitikai kémia |
| Online Access: | http://acta.bibl.u-szeged.hu/56107 |
| LEADER | 01763naa a2200253 i 4500 | ||
|---|---|---|---|
| 001 | acta56107 | ||
| 005 | 20220808154843.0 | ||
| 008 | 181212s2016 hu o 1|| zxx d | ||
| 020 | |a 978-963-306-507-5 | ||
| 040 | |a SZTE Egyetemi Kiadványok Repozitórium |b hun | ||
| 041 | |a zxx | ||
| 100 | 1 | |a Gorica Vuković | |
| 245 | 1 | 0 | |a Polar pesticide analyses |h [elektronikus dokumentum] : |b validation of glyphosate determination in soil by LC-MS/MS / |c Gorica Vuković |
| 260 | |c 2016 | ||
| 300 | |a 323-326 | ||
| 490 | 0 | |a Proceedings of the International Symposium on Analytical and Environmental Problems |v 22 | |
| 520 | 3 | |a Although glyphosate is a heavily applied herbicide worldwide, the risk of environmental contamination through transport mechanisms of this substance is still not well documented and the methods for its analysis are usually very complex and nor sensitive enough. In the measurement procedure with LC-MS/MS, a negative mode was used. FMOC-Cl derivatized glyphosate ions were identified by the precise determination of their ion mass. The LOQ was 0.01 mg/kg, with recovery of 101.4±4.49% and linearity over 0.99. The obtain method demonstrates the sensitivity, which enables measurements of glyphosate soil as a matrix. The success of the new extraction method was confirmed by measuring spiked soil samples to control recovery, linearity, LOD and LOQ. | |
| 695 | |a Peszticid, Analitikai kémia | ||
| 700 | 0 | 1 | |a Vojislava Bursić |e aut |
| 700 | 0 | 1 | |a Miroslav Agarski |e aut |
| 700 | 0 | 1 | |a Tijana Zeremski |e aut |
| 700 | 0 | 2 | |a Đurović-Pejčev Rada |e aut |
| 710 | |a International Symposium on Analytical and Environmental Problems (22.) (2016) (Szeged) | ||
| 856 | 4 | 0 | |u http://acta.bibl.u-szeged.hu/56107/1/proceedings_of_isaep_2016_323-326.pdf |z Dokumentum-elérés |